Synthesis and adsorption properties, toward some heavy metal ions, of a new polystyrene‐based terpyridine polymer
Identifieur interne : 000223 ( Main/Exploration ); précédent : 000222; suivant : 000224Synthesis and adsorption properties, toward some heavy metal ions, of a new polystyrene‐based terpyridine polymer
Auteurs : Haythem A. Saadeh [Jordanie] ; Eman A. Abu Shairah [Jordanie] ; Noureddine Charef [Algérie] ; Mohammad S. Mubarak [Algérie]Source :
- Journal of Applied Polymer Science [ 0021-8995 ] ; 2012-05-15.
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Abstract
A novel polymeric ligand having 2,2′:6′,2″‐terpyridine as pendant group was prepared through a Williamson type etherification approach for the reaction between 4′‐hydroxy‐2,2′: 6′,2″‐terpyridine and the commercially available 4‐chloromethyl polystyrene. The chelating properties of the new polymer toward the divalent metal ions (Cu2+, Zn2+, Ni2+, and Pb2+) in aqueous solutions was studied by a batch equilibration technique as a function of contact time, pH, mass of resin, and concentration of metal ions. The amount of metal‐ion uptake of the polymer was determined by using atomic absorption spectrometry. Results of the study revealed that the resin exhibited higher capacities and a more pronounced adsorption toward Pb2+ and that the metal‐ion uptake follows the order: Pb2+ > Cu2+ > Zn2+ > Ni2+. The adsorption and binding capacity of the resin toward the various metal ions investigated are discussed. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2012
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DOI: 10.1002/app.34977
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Sci.</title><idno type="ISSN">0021-8995</idno><idno type="eISSN">1097-4628</idno><imprint><publisher>Wiley Subscription Services, Inc., A Wiley Company</publisher><pubPlace>Hoboken</pubPlace><date type="published" when="2012-05-15">2012-05-15</date><biblScope unit="volume">124</biblScope><biblScope unit="issue">4</biblScope><biblScope unit="page" from="2717">2717</biblScope><biblScope unit="page" to="2724">2724</biblScope></imprint><idno type="ISSN">0021-8995</idno></series><idno type="istex">54BB6C6127B45202A23B12FBF0CAD83CDFEA9CA7</idno><idno type="DOI">10.1002/app.34977</idno><idno type="ArticleID">APP34977</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0021-8995</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>2,2′:6′,2″‐terpyridine</term><term>FTIR</term><term>adsorption properties</term><term>divalent metal ions</term><term>thermogravemetric analysis (TGA)</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A novel polymeric ligand having 2,2′:6′,2″‐terpyridine as pendant group was prepared through a Williamson type etherification approach for the reaction between 4′‐hydroxy‐2,2′: 6′,2″‐terpyridine and the commercially available 4‐chloromethyl polystyrene. The chelating properties of the new polymer toward the divalent metal ions (Cu2+, Zn2+, Ni2+, and Pb2+) in aqueous solutions was studied by a batch equilibration technique as a function of contact time, pH, mass of resin, and concentration of metal ions. The amount of metal‐ion uptake of the polymer was determined by using atomic absorption spectrometry. Results of the study revealed that the resin exhibited higher capacities and a more pronounced adsorption toward Pb2+ and that the metal‐ion uptake follows the order: Pb2+ > Cu2+ > Zn2+ > Ni2+. The adsorption and binding capacity of the resin toward the various metal ions investigated are discussed. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2012</div></front></TEI><affiliations><list><country><li>Algérie</li><li>Jordanie</li></country></list><tree><country name="Jordanie"><noRegion><name sortKey="Saadeh, Haythem A" sort="Saadeh, Haythem A" uniqKey="Saadeh H" first="Haythem A." last="Saadeh">Haythem A. Saadeh</name></noRegion><name sortKey="Shairah, Eman A Abu" sort="Shairah, Eman A Abu" uniqKey="Shairah E" first="Eman A. Abu" last="Shairah">Eman A. Abu Shairah</name></country><country name="Algérie"><noRegion><name sortKey="Charef, Noureddine" sort="Charef, Noureddine" uniqKey="Charef N" first="Noureddine" last="Charef">Noureddine Charef</name></noRegion><name sortKey="Mubarak, Mohammad S" sort="Mubarak, Mohammad S" uniqKey="Mubarak M" first="Mohammad S." last="Mubarak">Mohammad S. Mubarak</name><name sortKey="Mubarak, Mohammad S" sort="Mubarak, Mohammad S" uniqKey="Mubarak M" first="Mohammad S." last="Mubarak">Mohammad S. Mubarak</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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